| Title | Determination of trace elements in twenty six Chinese geochemistry reference materials by inductively coupled plasma-mass spectrometry |
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| Author | Liang, Q; Grégoire, D C |
| Source | Geostandards Newsletter vol. 24, no. 1, 2000 p. 51-63, https://doi.org/10.1111/j.1751-908x.2000.tb00586.x |
| Links | Abstract - Résumé
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| Year | 2000 |
| Alt Series | Geological Survey of Canada, Contribution Series 20070636 |
| Publisher | Wiley-Blackwell |
| Document | serial |
| Lang. | English |
| Media | paper; on-line; digital |
| File format | pdf |
| Subjects | geochemistry; trace elements; spectrometric analyses; mass spectrometer analysis; geochemical interpretations; analytical methods; rare earths; rare earths geochemistry |
| Illustrations | tables; plots |
| Released | 2007 05 22 |
| Abstract | We report new data for thirty seven elements determined in twenty six Chinese geochemistry reference materials using inductively coupled plasma?mass spectrometry and a reliable and simple dissolution
technique. One hundred milligrams of sample were digested with 1 ml of HF and 0.5 ml of HNO3 in PTFE?lined stainless steel bombs heated to 200 °C for 12 hours. Insoluble residues were dissolved using 6 ml of 40% v/v HNO3 heated to 140 C for 3 hours.
Analytical calibration was accomplished using aqueous standard solutions. Rhodium was used as an internal standard to correct for matrix effects and instrument drift. Precisions were typically better than 5% RSD. Most of the data presented here agree
well with the published certified values. For the elements Zr, Hf and most other trace elements, the measured values were less than 10% in error when compared to certified values. |
| GEOSCAN ID | 225029 |
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