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TitleRadiogenic Age and Isotopic Studies: Report 1
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LicencePlease note the adoption of the Open Government Licence - Canada supersedes any previous licences.
AuthorGeological Survey of Canada
SourceGeological Survey of Canada, Paper no. 87-2, 1987, 212 pages, https://doi.org/10.4095/122737 Open Access logo Open Access
Image
Year1987
Documentserial
Lang.English
Mediapaper; on-line; digital
RelatedThis publication contains the following publications
File formatpdf
ProvinceBritish Columbia; Alberta; Saskatchewan; Manitoba; Ontario; Quebec; New Brunswick; Nova Scotia; Prince Edward Island; Newfoundland and Labrador; Northwest Territories; Yukon; Nunavut; Canada
NTS1; 2; 3; 10; 11; 12; 13; 14; 15; 16; 20; 21; 22; 23; 24; 25; 26; 27; 28; 29; 30; 31; 32; 33; 34; 35; 36; 37; 38; 39; 40; 41; 42; 43; 44; 45; 46; 47; 48; 49; 52; 53; 54; 55; 56; 57; 58; 59; 62; 63; 64; 65; 66; 67; 68; 69; 72; 73; 74; 75; 76; 77; 78; 79; 82; 83; 84; 85; 86; 87; 88; 89; 92; 93; 94; 95; 96; 97; 98; 99; 102; 103; 104; 105; 106; 107; 114O; 114P; 115; 116; 117; 120; 340; 560
Subjectsgeochronology; radiometric dates; isotopic studies
Released1988 04 01; 2013 10 25
AbstractAnalytical procedures for V-Pb isotope dilution analyses at the Geological Survey of Canada geochronol­ogy laboratory are described in detail. The procedures apply to zircon, monazite, sphene, rutile, bad­deleyite, thorite, apatite, allanite, and gamet. Zircon in particular is carefully selected and generally air abraded, and is characterized using polishing and etching techniques. Reagent preparation and chemical processing are done in a clean air laboratory. Samples are spiked with a mixed 205Pb-233V-235V tracer, dissolved using steel jacketed Teflon pressure vessels or TeflonTM screw cap containers. U and Pb are separated using anion exchange resin columns. Blanks for typical sample amounts of O. 01 to 1. 0mg are less than J0pg V and 6-40pg Pb. Rapid JO minute mass analysis of the V and Pb are carried out using a Finnigan MAT 261 variable multicollector mass spectrometer solely in the static mode. Data reduction incorporates consideration of all sources of error in the analysis, and discordant V-Pb results are assessed on concordia plots using published regression techniques, taking into consideration the particular mineral systematics.
GEOSCAN ID122737

 
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